PUREPATH 100 Distillation System
Item No: PUREPATH 100
- Cascade’s PUREPATH 100 is a 4″ wiped film distillation package optimized for viscous crude refinement. The PUREPATH features top quality components from Agilent, Asahi, Heidolph, and Huber.
- Requires dry ice for cold trap (Upgrade anytime to KIT A for Huber Mechanically Refrigerated Cold Traps!)
- Fused electrical box allows system to run on single 50AMP 1ph 120V-240V service
- Modular system allows for expansion
- All tubing, fluids, connections included
- NRTL listed components
Call or Chat with our experts about upgrading to Kit A and pricing!
The PUREPATH Difference
There are a number of different distillation systems on the market. Cascade’s PUREPATH 100 has a few marked differences.
1) Temperature Delta Of Asahi Glass Helps Minimize Breakage
The truth is – glass breaks and the distillation glassware is expensive to replace. The Asahi Glass on the PUREPATH has an industry leading 110°C temperature delta. This means the Asahi Glass on the PUREPATH can withstand the temperature shocks associated with rapid, hot to cold temperature changes that could occur with extreme temperature ranges – or when cold ethanol is introduced into the system to clean.
2) Keep It Clean! The Vacuum Integrity Of The Asahi Glass Is Exceptional – Seals And Joints Do Not Require Grease
Many products manufactured in a distillation system are destined for human consumption. The PUREPATH seals and joints are super smooth, which not only means exceptional vacuum integrity, but that you won’t have to introduce grease into the system in order to maintain vacuum. Lesser quality glass will often slightly leak – reducing performance/output and increase labor efforts chasing down small vacuum leaks.
3) The Vacuum Pumping System – Deep, Protected From Contamination & Real Time Graphical Data
The vacuum system features a UL Listed Agilent DS302 Rotary Vane Pump Since the vacuum integrity of the Asahi Glass is so strong, it clears the way for the vacuum pump to get deeper to its ultimate pressure of 2×10-3 mbar. We protect and keep processing clean with a foreline trap on the inlet and an oil mist return.
4) Rodaviss® Couplings For Easy, Safe Disconnect Of Receiving Flasks
Cascade’s PUREPATH minimizes another potential glass break point by utilizing Rodaviss couplings.
5) Professional on-site installation and training. Our installation and training crew is a team of technicians from Cascade Sciences, Asahi Glass and seasoned industry veterans.
Straight Talk About Thru-Put
There are many variables that dictate thru put of any wiped film system. Crude oil will run through at different rates.
To produce quality distillate, crude oil typically must run through the system twice.
• 1st Run strips terpenes and volatiles (Heads)
• 2nd Run distills heavy cannabinoids (Body)
Benefits of the PUREPATH 100 include:
• High Evaporation Efficiency
• Minimum Thermal Decomposition
• Gas and Vacuum Tight
• Uniform Thin Film
• Jacketed Evaporator for Easy Viewing
• Uniform Rotating Wiper System (Up to 300°C Option)
• Grease-less Magnetic Sealed Bearing, Valve and Joints
• Perfect for Heat Sensitive Materials
• Short Residence Time
Asahi Glass
• Jacketed Evaporator ID 100mm with evaporation surface area of 0.1m2
• Receiver 1000ml, Borosilicate Glass 3.3
• Temperature range of glass –90°C to +230°C
• Delta of Glass 110°C (the temperature change the glass can withstand without breaking)
• 2L Feed Vessel includes vent valve, thermometer pocket, cap, needle valve
• External Condenser: Thermal transfer area 0.2m2 with 2 water connectors
• Magnetic Seal with Cover –torque 1.1Nm / Cover SS316
• Wiper: PTFE Wiper +200°C
• Overall Design Operating Pressure 0.1 mbar
• Cold Finger: Dry Ice capacity of up to 475ml
Huber Temperature Control
Huber 202 Heating Feed Vessel with Temperature Probe
General information & temperature controller
• Temperature range: 45°C to 200°C
• Temperature stability: ±0.02°C
• Temperature control: TAC, self-optimizing (True Adaptive Control)
• Controller: Pilot ONE (E-grade “Basic”)
• Safety class: III / FL
• Protection class: IP20
• Dimensions: 7″W x 10.2″D x 13.9″H
• Weight: 8kg
Heating / cooling capacity
• Heating capacity: 2kW
Circulation pump
• Pressure pump max.: 27 l/min ; 0,7 bar
• Suction pump max.: 22 l/min ; 0,4 bar
• Pump connection: M16x1 AG male
Connections
• Pt100 connection: Pt100
• Digital interface: RS232, Ethernet, USB Device, USB Host
Operating data
• Permissible ambient temp.: 5…40°C
• Bath opening WxD/BD: Ø = 25 / 150 mm
• Bath volume: 2L
• Power supply: 230V 1~ 50/60Hz
• Current max.: 10 A
Huber 125 Ministat Cooling Main Body Condenser
General information & temperature controller
• Temperature range: -25°C to 150°C
• Temperature stability: ±0.02°C
• Temperature control: TAC, self-optimizing (True Adaptive Control)
• Controller: Pilot ONE (E-grade “Basic”)
• Safety class: III / FL
• Protection class: IP20
• Dimensions: 8.9″W x 14.6″D x 16.9″H
• Weight: 25kg
Heating / cooling capacity
• Heating capacity: 1.5kW
• Cooling capacity:
100 20 0 -10 -20 °C
0.3 0.3 0.21 0.15 0.05 kW
• Cooling machine: air-cooled
• Refrigerant: R290 (0.1kg)
Circulation pump
• Pressure pump max.: 22 lpm ; 0.7 bar | 5.81 gpm ; 10.15 psi
• Suction pump max.: 16 lpm ; 0.4 bar | 4.23 gpm ; 5.8 psi
• Pump connection: M16x1 AG male
• Permissible viscosity: 50 mm²/s
Connections
• Pt100 connection: Pt100
• Digital interface: RS232, Ethernet, USB Device, USB Host
Operating data
• Permissible ambient temp.: 5°C to 35°C
• Noise Level: 47dB(A)
• Bath opening W x D / BD: 178 x 80 / 120 mm
• Bath volume: 2.75L
• Filling volume min.: 2L
• Power supply: 115V 1~ 50/60Hz
• Current max.: 11.5 A
Huber 304 Heating Main Body Jacket
General information & temperature controller
• Temperature range: 28°C to 300°C
• Temperature stability: ±0.02°C
• Temperature control: TAC, self-optimizing (True Adaptive Control)
• Controller: Pilot ONE (E-grade “Basic”)
• Safety class: III / FL
• Protection class: IP20
• Dimensions: 8.3″W x 13.1″D x 15.4″H
• Weight: 14kg
Heating / cooling capacity
Heating capacity: 3kW
Circulation pump
• Pressure pump max.: 25 l/min ; 0,7 bar
• Suction pump max.: 18.5 l/min ; 0,4 bar
• Pump connection: M16x1 AG male
• Permissible viscosity: 50 mm²/s
Connections
• Pt100 connection: Pt100
• Digital interface: RS232, Ethernet, USB Device, USB Host
Operating data
• Permissible ambient temp.: 5…40°C
• Bath opening WxD/BD: 130 x 100 / 155mm
• Bath volume: 5L
• Filling volume minimum: 3.2L
• Power supply: 230V 1~ 50/60Hz
• Current max.: 14A
• Fusing: 16A
Agilent Vacuum Power
Agilent DS302 8.2 CFM
• Pump Type: Oil, Rotary Vane
• Pumping Speed: 8.2 CFM
• Ultimate Pressure: 2 × 10-3 mbar
• Power: 120V / 1ph (220V available)
• Intake Connection: KF-25
• Dimensions: 19.33″L x 5.27″W x 8.34″H
• Weight: 53lbs
Vacuum Gauges, Connection Hardware included
KIRK-1 FEATURES
• Auto Off
• On/Off soft switch
• Battery level indication
• Good/Bad sensor (tube) indication
• Self test mode
• Field replaceable sensor
• 3 different graphical displays of vacuum pressure (pump-down, line, or bar graph)
• Vacuum analytics for leak, outgassing and pump-down
Unit Size
• Length: 28″
• Width: 83″
• Height: 83″
Power Requirements
See attached facility power requirements PDF under MANUALS & VIDEOS TAB
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